Reference of 6793-92-6, These common heterocyclic compound, 6793-92-6, name is 1-Bromo-4-(phenylmethoxy)benzene, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Nanoporous metal gold catalyst (9.8 mg, 0.05 mmol), ethanol (2 mL) and 4-benzyloxybromobenzene(65.75 mg, 0.25 mmol), cesium carbonate (364.3 mg, 1.125 mmol) was added to the reaction kettle, and hydrogen (40 bar) was added.Heat stirring, the reaction temperature is controlled at 100 C, the reaction time is controlled at 90 h, and the reaction solution is extracted with water to obtain 42.32 mg of biphenyl.The yield was 92%.
Statistics shows that 1-Bromo-4-(phenylmethoxy)benzene is playing an increasingly important role. we look forward to future research findings about 6793-92-6.
Reference:
Patent; Dalian University of Technology; Bao Ming; Zhao Yuhui; Feng Xiujuan; Yu Xiaoqiang; Zhang Sheng; (13 pag.)CN109608297; (2019); A;,
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