Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 5414-19-7, name is 1-Bromo-2-(2-bromoethoxy)ethane, A new synthetic method of this compound is introduced below., Recommanded Product: 1-Bromo-2-(2-bromoethoxy)ethane
Compound 2b (100 mg) was reacted with bis(2-bromoethyl) ether(1.0 mL) in MeCN (10 mL) in the presence of K2CO3 (25 mg) and 18-crown-6-ether (7.4 mg) at 50 C for 5 h. Next, the reaction mixture was concentrated on a rotary evaporator and then poured into hexane to remove any unreacted bis(2-bromoethyl)ether. The precipitated crude product was purified by column chromatography on SiO2 with CHCl3-MeOH (100:120:1 v/v) as the eluent to provide 2c.
The synthetic route of 5414-19-7 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Matsumoto, Jin; Kubo, Tomoya; Shinbara, Tomohiko; Matsuda, Naomi; Shiragami, Tsutomu; Fujitsuka, Mamoru; Majima, Tetsuro; Yasuda, Masahide; Bulletin of the Chemical Society of Japan; vol. 86; 11; (2013); p. 1240 – 1247;,
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