Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 17715-69-4, name is 1-Bromo-2,4-dimethoxybenzene, This compound has unique chemical properties. The synthetic route is as follows., Computed Properties of C8H9BrO2
To a mixture ofl-bromo-2,4-dimethoxybenzene (72 jiL, 0.50 mmol, 1 equiv), cyclopropylboronic acid (64 mg, 0.75 mmol, 1.5 equiv), and K3PO4H2O (0.35 mg, 1.5 mmol, 3 equiv) was added toluene (400 iL) then a THF stock solution of 3 and PAd3 (100 iL, 0.25 iimol of Pd/PAd3) and the mixture was stirred at 100 C for 5 h. The reaction mixture was diluted withethyl acetate then extracted with water. The combine organic layers were evaporated and the crude product was purified by flash chromatography. After drying, 80 mg (90 %) of 23 was obtained as a colorless oil. NMR spectroscopic data agreed with literature values.
According to the analysis of related databases, 17715-69-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; THE TRUSTEES OF PRINCETON UNIVERSITY; CARROW, Brad P.; CHEN, Liye; (51 pag.)WO2017/75581; (2017); A1;,
Ether – Wikipedia,
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