Electric Literature of 7252-83-7,Some common heterocyclic compound, 7252-83-7, name is 2-Bromo-1,1-dimethoxyethane, molecular formula is C4H9BrO2, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
In a 250 mL round bottom flask was added 4-(morpholinyl)thiobenzamide (2.22 g, 10 mmol) and dissolved in ethanol (50 mL).Then 2-bromo-1,1-dimethoxyethane (1.69 g, 10 mmol) and p-toluenesulfonic acid (1.90 g, 10 mmol) were added while stirring, and the reaction system was heated to 95C and reacted overnight.After the reaction was completed, the mixture was cooled to room temperature and filtered to give a solid which after drying gave a yellow solid (2.00 g, 81%).
The synthetic route of 7252-83-7 has been constantly updated, and we look forward to future research findings.