Totally synthetic steroid hormones. V. (±)-2,3-Dimethoxyestra-1,3,5(10)-trien-17β-ol and some congeners was written by Douglas, G. H.;Walk, C. R.;Smith, Herchel. And the article was included in Journal of Medicinal Chemistry in 1966.Quality Control of 3-(3,4-Dimethoxyphenyl)propan-1-ol This article mentions the following:
(±)-2,3-Dimethoxy-1,3,5(10)-estratrien-17-one and -17β-ol have been totally synthesized from 6,7-dimethoxy-1-tetralone. Their estrogenic and blood cholesterol lowering properties are recorded. In the experiment, the researchers used many compounds, for example, 3-(3,4-Dimethoxyphenyl)propan-1-ol (cas: 3929-47-3Quality Control of 3-(3,4-Dimethoxyphenyl)propan-1-ol).
3-(3,4-Dimethoxyphenyl)propan-1-ol (cas: 3929-47-3) belongs to ethers. Relative to alcohols, ethers are generally less dense, are less soluble in water, and have lower boiling points. They are relatively unreactive. Autoxidation is the spontaneous oxidation of a compound in air. In the presence of oxygen, ethers slowly autoxidize to form hydroperoxides and dialkyl peroxides. If concentrated or heated, these peroxides may explode. To prevent such explosions, ethers should be obtained in small quantities, kept in tightly sealed containers, and used promptly.Quality Control of 3-(3,4-Dimethoxyphenyl)propan-1-ol
Referemce:
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem