Patil, Rupesh C.; Jagdale, Ashutosh A.; Patil, Uttam P.; Ghodake, Jeevan S.; Mali, Sawanta S.; Hong, Chang K.; Patil, Suresh S. published their research in Catalysis Letters in 2021. The article was titled 《Agro-Waste Generated Pd/CAP-Ash Catalyzed Ligand-Free Approach for Suzuki-Miyaura Coupling Reaction》.Quality Control of 1-Bromo-3-methoxybenzene The article contains the following contents:
We converted agro-waste custard apple peels (CAP) to ash via thermal treatment, on which Pd(OAc)2 was immobilized easily that produced a low-cost, highly efficient Pd/CAP-ash catalyst. The prepared catalyst was fully characterized by using FT-IR, SEM, EDX, XRF, DSC-TGA, BET, HR-TEM, and XPS techniques. The Pd/CAP-ash catalyst was conveniently applied for the Suzuki-Miyaura coupling reaction under external base free and ligand-free conditions in an aqueous-organic solvent to produce biphenyls in good to excellent yields. The main attraction of our protocol an application of palladium-supported agro-waste material which is easily recoverable and recyclable provides mono and bis-coupled derivatives in a short reaction time. The experimental process involved the reaction of 1-Bromo-3-methoxybenzene(cas: 2398-37-0Quality Control of 1-Bromo-3-methoxybenzene)
1-Bromo-3-methoxybenzene(cas: 2398-37-0) is a compound useful in organic synthesis and other chemical processes. It is an intermediate used for pharmaceuticals, perfumes and agrochemicals.Quality Control of 1-Bromo-3-methoxybenzene
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