Extracurricular laboratory: Synthetic route of 73590-85-9

The article 《13C Satellite-Free 1H NMR Spectra》 also mentions many details about this compound(73590-85-9)Synthetic Route of C17H19N3O2S, you can pay attention to it, because details determine success or failure

Synthetic Route of C17H19N3O2S. Aromatic compounds can be divided into two categories: single heterocycles and fused heterocycles. Compound: 5-Methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridyl)methyl]thio]benzimidazole, is researched, Molecular C17H19N3O2S, CAS is 73590-85-9, about 13C Satellite-Free 1H NMR Spectra. Author is Moutzouri, Pinelopi; Kiraly, Peter; Phillips, Andrew R.; Coombes, Steven R.; Nilsson, Mathias; Morris, Gareth A..

A new NMR experiment (Destruction of Interfering Satellites by Perfect Echo Low-pass filtration, DISPEL) is introduced that facilitates the anal. of low-level components in high dynamic range mixtures by suppressing one-bond 13C satellite signals in 1H spectra. Since the natural abundance of 13C is around 1.1%, these satellites appear at 0.54% of the intensity of a parent peak, mimicking and often masking impurity signals. The new experiment suppresses one-bond 13C satellite signals, with high efficiency, at negligible cost in signal-to-noise ratio, and over a wide range of one-bond coupling constants, without the need for broadband 13C decoupling.

The article 《13C Satellite-Free 1H NMR Spectra》 also mentions many details about this compound(73590-85-9)Synthetic Route of C17H19N3O2S, you can pay attention to it, because details determine success or failure

Reference:
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem