In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 103-50-4, name is Benzyl ether belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. category: ethers-buliding-blocks
General procedure: A mixture of azobenzene 1 (0.25 mmol), dibenzyl ether 2 (0.75 mmol), TBHP (1.5 mmol), and DCE (1 mL) was charged into a sealed tube. After stirring vigorously at 120 C for 24 h, the mixture was evaporated under vacuum. The corresponding product 7 was isolated by silica gel column chromatography with a PE/EtOAc mixture as eluent.
The synthetic route of 103-50-4 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Hong, Gang; Aruma, Alfred Njasotapher; Zhu, Xiaoyan; Wu, Shengying; Wang, Limin; Synthesis; vol. 48; 8; (2016); p. 1147 – 1158;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem