Related Products of 707-07-3, These common heterocyclic compound, 707-07-3, name is (Trimethoxymethyl)benzene, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Example 6 To a mixture of 16.6 g of compound according to example 2 in toluene (600 ml) trimethyi ortobenzoate (120 ml) and camphenesulphonic acid (4 g) were added. The mixture was stirred vigorously at rt for 3 h, then 80 % acetic acid (160 ml) was added. After further 1 h of stirring the biphasic mixture obtained was separated, the organic phase was diluted with toluene (600 ml), washed with water (800 ml) and sat. NaHC03 (2 x 600 ml), dried, filtered and evaporated. The resulting oil was dropped into 600 ml of heptane and seeded. The white crystalline compound was filtered, washed and dried to yield 1 10.3 g of acceptor (a compound of general formula 6, wherein R|= Bn, R2= 4-chlorobenzoyl, R3= benzoyl, ORj in beta). [a]D = +17.13 (c = 1 DCM), Mp 156-157 C.
Statistics shows that (Trimethoxymethyl)benzene is playing an increasingly important role. we look forward to future research findings about 707-07-3.
Reference:
Patent; GLYCOM A/S; BAJZA, Istvan; DEKANY, Gyula; AGOSTON, Karoly; PEREZ, Ignacio Figueroa; BOUTET, Julien; HEDEROS, Markus; HORVATH, Ferenc; KOVACS-PENZES, Piroska; KROeGER, Lars; ROeHRIG, Christoph; SCHROVEN, Andreas; VRASIDAS, Ioannis; TRINKA, Peter; KALMAR, Laszlo; KOVACS, Imre; DEMKO, Sandor; AGOSTON, Agnes; RISINGER, Christian; WO2011/100980; (2011); A1;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem