Reference of 1836-62-0, The chemical industry reduces the impact on the environment during synthesis 1836-62-0, name is 2-(2-Methoxyphenoxy)ethylamine, I believe this compound will play a more active role in future production and life.
To a solution of benzyl bromide (4100 mg, 23.92 mmol) in toluene(15 ml) was added triethylamine (6051 mg, 59.80 mmol)the temperature was lowered to 0 C .Toluene (10 ml) in which 2-(2-methoxyphenoxy)ethanamine (5000 mg, 29.90 mmol) was slowly added dropwise at 0 C,The temperature was increased to 25 C . After the reaction mixture was stirred at room temperature for 8 hours, water (25 ml) was added dropwise to the reaction mixture, and the mixture was stirred for 15 minutes. The organic layer was then separated, washed with water (15 ml), dried over sodium sulfate and concentrated in vacuo to give the crude product. The crude product was then purified by column chromatography on silica gel, 15-80% ethyl acetate / hexane to give the final compound as the final product.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-(2-Methoxyphenoxy)ethylamine, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Gachon University Industry Academy Cooperation Foundation; Kim Mi-hyeon; Kim Seon-yeo; Jang Cheong-yun; (29 pag.)KR2018/125090; (2018); A;,
Ether – Wikipedia,
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