Reference of 24599-58-4, The chemical industry reduces the impact on the environment during synthesis 24599-58-4, name is 2,5-Dimethoxytoluene, I believe this compound will play a more active role in future production and life.
General procedure: Standard reaction conditions: a 1.0 mmol sample of the aryl ether was dissolved in 1.8mL of acetonitrile and was added slowly over several minutes to a rapidly stirred solution of CAN (1.92g, 3.5mmol) which had been dissolved in 1.8 mL of distilled water in a 10mL round-bottom flask. After the addition was complete, the mixture was stirred for an additional 1 hour at room temperature open to the air. The mixture was diluted with 25 mL of water, and the resulting precipitate collected by suction filtration. The precipitate was washed with several 10 mL portions of water and then finally with approximately 5mL of ice cold ethanol. The resulting yellow solid (diquinone) was dried at room temperature under vacuum.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2,5-Dimethoxytoluene, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Love, Brian E.; Simmons, Alexander L.; Tetrahedron Letters; vol. 57; 50; (2016); p. 5712 – 5715;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem