Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 36805-97-7, name is 1,1-Di-tert-butoxy-N,N-dimethylmethanamine, A new synthetic method of this compound is introduced below., HPLC of Formula: C11H25NO2
Example 3; Ethyl 6-[(dimethylamino)methylene]-l-methyl-7-oxo-4,5,6,7-tetrahydro-lH- indazole-3-carboxylate; 16 g (72 mmol) of ethyl l-methyl-7-oxo-4,5,6,7-tetrahydro-lH-indazole-3- carboxylate were dissolved in 100 mL of dimethylformamide and 32 mL of dimethylformamide ditertbutyl acetale were added. The mixture was stirred at 600C for 8 hours. The solvent was then evaporated in vacuo and the product crystallized from ethanol to give the title compound (17.96 g, 90 % yield). 1H NMR (400 MHz, DMSO-J6) delta ppm 1.31 (t, J= 7.07 Hz, 3 H) 2.83 (m, 2 H) 2.92 (m, 2 H) 3.13 (s, 6 H) 4.14 (s, 3 H) 4.24 (q, J= 7.07 Hz, 2 H) 7.49 and 7.52 (2 s, 1 H).
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; NERVIANO MEDICAL SCIENCES S.r.l.; WO2008/74788; (2008); A1;,
Ether – Wikipedia,
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