Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 1836-62-0, name is 2-(2-Methoxyphenoxy)ethylamine, A new synthetic method of this compound is introduced below., SDS of cas: 1836-62-0
General procedure: Synthetic method: 1-alkyl-2-methyl-5-hydroxy-1H-indole-3-carboxylic acid 0.020 mol, O-methoxyphenoxyethylamine (12.16 g, 0.060 mol), N, N-dimethylformamide 10 mL and dichloromethane 100 mL were placed in a 250 mL eggplant flask, The HOBt (4.05 g, 0.030 mol), Triethylamine (6.07 g, 0.060 mol) EDCI (5.75 g, 0.030 mol) were added thereto, respectively, The reaction was stirred at room temperature for 16 h, The reaction solution was washed with a 2 mol / L aqueous hydrochloric acid solution and a saturated sodium bicarbonate solution, Add a large amount of water to stir the precipitated solid, Filter, Product crude ethanol recrystallization.
The synthetic route of 1836-62-0 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shenyang Pharmaceutical University; Hu Chun; Zhang Lan; Ke Jia; Jin Zhe; Yao Dongming; Guo Wanxin; Liu Xiaoping; (35 pag.)CN106946761; (2017); A;,
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