Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 36805-97-7, name is 1,1-Di-tert-butoxy-N,N-dimethylmethanamine, This compound has unique chemical properties. The synthetic route is as follows., Quality Control of 1,1-Di-tert-butoxy-N,N-dimethylmethanamine
[0403] To a solution of 5-acetyl-N-(2,6-diethylphenyl)-1-methyl-1H-pyrazole-3-carboxamide (0.013 g, 0.043 mmol) in DMF (1.5 mL), N,N-dimethylformamide di-tertbutyl acetal (0.0.63 mL, 0.650 mmol) was added. The mixture was stirred at 80 C. for 2 h. The reaction was diluted with water, extracted with AcOEt (2×20 mL). The organic fractions were combined, dried over Na2SO4, filtered, and concentrated in vacuo and the residue used without any further purification. (0.017 g, 78% yield). [0404] 1H NMR (400 MHz, DMSO-d6) delta ppm 9.58 (s, 1H), 7.71 (d, J=12.33 Hz, 1H), 7.36 (s, 1H), 7.21 (t, J=7.60 Hz, 1H), 7.12 (d, J=7.60 Hz, 2H), 5.75 (d, J=12.33 Hz, 1H), 4.18 (s, 3H), 3.16 (s, 3H), 2.92 (s, 3H), 2.52 (q, J=7.57 Hz, 4H), 1.09 (t, J=7.57 Hz, 6H) [0405] HRMS (ESI) calcd for C20H27N4O2 [M+H]+ 355.2129. found 355.2133.
According to the analysis of related databases, 36805-97-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; NERVIANO MEDICAL SCIENCES S.R.L.; Casuscelli, Francesco; Brasca, Maria Gabriella; Caldarelli, Marina; Cervi, Giovanni; Disingrini, Teresa; Quartieri, Francesca; US2014/51708; (2014); A1;,
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