Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 10541-78-3, name is 2-Methoxy-N-methylaniline, This compound has unique chemical properties. The synthetic route is as follows., Quality Control of 2-Methoxy-N-methylaniline
General procedure: The N-methyl aniline intermediates were prepared according to the method in the literature. To a solution of sodium 3,4-dioxo-3,4-dihydronaphthalene-1-sulfonate (2) (130 mg, 0.5 mmol) in water (15 mL), N-methyl aniline intermediate (0.55 mmol) was added. The reaction mixture was stirred at room temperature for 3 to 20 h (TLC monitoring). For the preparation of compounds 3, the solvent was removed in vacuum, and the residue was purified by column chromatography to give the target products. For the preparation of compounds 4, the precipitate produced was filtered, and the residue was crystallized from EtOH to give compounds 4 as red solids.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 10541-78-3.
Reference:
Article; Yang, Honghao; An, Baijiao; Li, Xingshu; Zeng, Wei; Bioorganic and Medicinal Chemistry Letters; vol. 28; 18; (2018); p. 3057 – 3063;,
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