Application of 2930-05-4, The chemical industry reduces the impact on the environment during synthesis 2930-05-4, name is 2-((Benzyloxy)methyl)oxirane, I believe this compound will play a more active role in future production and life.
General procedure: To a 4 mL of vial was charged with [Bmim]Br (43.8 mg, 0.2 mmol), NaHCO3 (8.4 mg, 0.1 mmol), LiCl (4.2 mg, 0.1 mmol), epoxide (2 mmol) and CS2 (364 mL, 6 mmol). The reaction mixture was stirred at 40 C for 24 h, after which time, water (5 mL) was added into the reaction mixture. The organic layer was extracted with CH2Cl2 (3 x 5 mL). The combined organic phase was dried over anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by flash column chromatography on silica gel (petroleum ether/ethyl acetate = 4:1 as eluent).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-((Benzyloxy)methyl)oxirane, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Mei, Congmin; Li, Xu; Liu, Lihuai; Cao, Changsheng; Pang, Guangsheng; Shi, Yanhui; Tetrahedron; vol. 73; 38; (2017); p. 5706 – 5714;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem