Synthetic Route of 22483-09-6, The chemical industry reduces the impact on the environment during synthesis 22483-09-6, name is 2,2-Dimethoxyethanamine, I believe this compound will play a more active role in future production and life.
Compound 3 (1.0 g, 6.82 mmol) was dissolved in aqueous NaOH (0.275 g in 20 ml water) to yield a clear solution. Aminoacetaldehyde dimethyl acetal (0.93 ml, 8.58 mmol) was added. The mixture was placed on an oil bath (120-130 C); foaming lasted for 3 h. The mixture was cooled. The resulting grey powder was recovered by filtration, washed with cold water, and dried under high vacuum to give 4 (yield 1.3 g, 88%). 1H NMR (D2O): 2.79 (s, 2H), 2.81 (s, 6H), 3.99 (t, J =5.4 Hz, 1H).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2,2-Dimethoxyethanamine, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Laos, Roberto; Lampropoulos, Christos; Benner, Steven A.; Acta Crystallographica Section C: Structural Chemistry; vol. 75; 1; (2019); p. 22 – 28;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem