Reference of 150-78-7, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 150-78-7 as follows.
[00328] FIG. 33 illustrates the synthetic pathway to create DPB A-TPE. [00329] To demonstrate the potential of AIE dots for cellular and mitochondria dual targeted image-guided PDT, we synthesized a new AIEgen, DPBA-TPE (FIG. 33). 3,3′-(2,5- Dimethoxy-l,4-phenylene)bis(2-(4-bromophenyl)acrylonitrile) (5) was prepared by Knoevenagel reaction from 2,5-dimethoxybenzene-l ,4-dicarboxaldehyde (3) and bromophenylacetonitrile (4) under basic conditions. The final product was obtained with satisfactory yields by intermediate (5) and aryl amine (10) in the presence of palladium catalyst under basic conditions.
According to the analysis of related databases, 150-78-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; NATIONAL UNIVERSITY OF SINGAPORE; THE HONG KONG UNIVERSITY OF SCIENCE AND TECHNOLOGY; LIU, Bin; YUAN, Youyong; FENG, Guangxue; TANG, Ben Zhong; QIN, Wei; ZHANG, Chongjing; XU, Shidang; WO2015/163817; (2015); A1;,
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