Related Products of 6346-09-4, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 6346-09-4, name is 4,4-Diethoxybutan-1-amine belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
To a solution of appropriate amine (11.2 mmol) in dry CH2Cl2 (11 ml) CDI (2.0 g, 12.3 mmol) wasadded. The mixture was stirred at room temperature for 120 h. To the resulting solution 4,4-diethoxybutyl-1-amine (1.80 g, 11.2 mmol) was added and the reaction mixture was stirred at roomtemperature for additional 72 h. Solvent was evaporated invacuo. Residue was througly washedwith water, filtered and dried in vacuo (2 h, 0.01 torr) to give the title compound 1.
The synthetic route of 4,4-Diethoxybutan-1-amine has been constantly updated, and we look forward to future research findings.
Reference:
Article; Gazizov; Smolobochkin; Voronina; Burilov; Pudovik; Tetrahedron; vol. 71; 3; (2015); p. 445 – 450;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem