These common heterocyclic compound, 1663-61-2, name is (Triethoxymethyl)benzene, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route. name: (Triethoxymethyl)benzene
General procedure: Triethyl orthoformate, orthoacetate, orthopropionate or orthobenzoate(10 mmol) was added dropwise to the mixture of 1,2,4,5-tetrazine-3,6-dicarbohydrazide (6) (0.5 g, 2.5 mmol) and glacial aceticacid (7 mL). The reaction was carried out using conventional heating ormicrowave irradiation (150 W) in five cycles of 90 s with 2 min intervalsat the temperature 50-100 C.
The synthetic route of (Triethoxymethyl)benzene has been constantly updated, and we look forward to future research findings.
Reference:
Article; K?dzia, Anna; Kudelko, Agnieszka; ?wi?tkowski, Marcin; Kruszy?ski, Rafa?; Dyes and Pigments; vol. 172; (2020);,
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