Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 111-95-5, name is Bis(2-methoxyethyl)amine, This compound has unique chemical properties. The synthetic route is as follows., Quality Control of Bis(2-methoxyethyl)amine
To an ethanolic solution (50 ml) of p-chlorophenol (30 mmol, 3.86 g), bis(2-methoxyethyl)amine (30 mmol, 3.99 g) was added dropwise with constant stirring. After 30 min, 37% (w/v) formalin solution (30 mmol, 2.43ml) was added to it. The resulting mixture was stirred for 1 h at room temperature and then refluxed for 8 h. It was evaporated under reduced pressure and the yellow oil was extracted with saturated brine solution and diethyl-ether several times. The organic phase was separated, dried with anhydrous MgSO4, concentrated by evaporation of ether and subsequently vacuum-dried for the removal of last traces of water.
According to the analysis of related databases, 111-95-5, the application of this compound in the production field has become more and more popular.
Reference:
Article; Sanyal, Ria; Chakraborty, Prateeti; Zangrando, Ennio; Das, Debasis; Polyhedron; vol. 97; (2015); p. 55 – 65;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem