Extracurricular laboratory: Synthetic route of 1-(4-Methoxyphenyl)ethylamine

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 6298-96-0, name is 1-(4-Methoxyphenyl)ethylamine, A new synthetic method of this compound is introduced below., Product Details of 6298-96-0

General procedure: The appropriate amine derivative was dissolved in the appropriate solvent (ethanol or pyridine) after which CS2 was added. The mixture was refluxed overnight under N2. Next, the solution was concentrated by evaporating the solvent and then cooled to give aprecipitate. The precipitated product was isolated by vacuum filtration. The crude N,N’-bis-thiourea was purified by recrystallizationfrom ethanol.

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Reference:
Article; Tuncel, Senel Teke; Gunal, Sule Erol; Ekizoglu, Melike; Gokhan Kelekci, Nesrin; Erdem, Safiye S.; Bulak, Ece; Frey, Wolfgang; Dogan, Ilknur; Journal of Molecular Structure; vol. 1179; (2019); p. 40 – 56;,
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