Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 10075-63-5, name is 1,5-Dimethoxynaphthalene, A new synthetic method of this compound is introduced below., Recommanded Product: 10075-63-5
70% Nitric acid (4.5 mL) in acetic acid (4.5 mL) was added slowly to a stirred suspension of 1,5-dimethoxynaphthalene(3.76 g, 20 mmol) in acetic acid (50 mL)at room temperature. Upon stirring overnight at ambienttemperature, the precipitate was filtered off,washed with water, recrystallized from methanol, anddried. Light yellow solid, yield 82%. 1H NMRspectrum, delta, ppm: 3.91 s (6H), 7.31 d (J = 8.5 Hz, 2H), 8.01 d (J = 8.5 Hz, 2H). 13C NMR spectrum, delta, ppm:57.45, 107.87, 116.85, 124.51, 140.69, 155.01.
The synthetic route of 10075-63-5 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Dong; Zhang; Huang; Meng; Li; Russian Journal of General Chemistry; vol. 87; 4; (2017); p. 837 – 841; Zh. Obshch. Khim.; vol. 87; 4; (2017); p. 837 – 841,5;,
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