Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 57602-02-5, name is 1,14-Dibromo-3,6,9,12-tetraoxatetradecane, A new synthetic method of this compound is introduced below., Safety of 1,14-Dibromo-3,6,9,12-tetraoxatetradecane
General procedure: Thioacetate 3 (2.2 eq) and dibromide (1eq) were dissolved in dry DMF. DEA was added dropwise and the reaction was stirred for 3 h at room temperature. Then the reaction mixture was washed with 1 M HCl (aq), extracted with CH 2Cl 2, dried with Na 2SO 4. The solution was concentrated and purified by column chromatography.
The synthetic route of 57602-02-5 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Yang, Yang; He, Yun; Li, Xingzhe; Dinh, Hieu; Iyer, Suri S.; Bioorganic and Medicinal Chemistry Letters; vol. 24; 2; (2014); p. 636 – 643;,
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