In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 17715-70-7 as follows. category: ethers-buliding-blocks
Example 15 Preparation of 4-fluororesorcinol (15) Using general method E, Compound 11 (27.4 g, 157.9 mmol) gives Compound 15 as 20.7 g (100%) of a colorless crystalline solid: m.p. 94-96 C.; 1 H-NMR (d6 -DMSO) 8.39 (br, 1H), 8.00 (br, 1H), 6.89 (dd, 1H), 6.48 (dd, 1H), 6.27 (ddd, 1H). 19 F-NMR (d6 -DMSO) 145.82 (m). Anal calc. for C6 H5 FO2: C, 56.26; H, 3.93. Found: C, 56.23; H, 3.93.
According to the analysis of related databases, 17715-70-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Molecular Probes, Inc.; US6162931; (2000); A;,
Ether – Wikipedia,
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