In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 2734-70-5, name is 2,6-Dimethoxyaniline belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Formula: C8H11NO2
Weigh 0.5 mmol of amide III-1, 1percent molar amount of palladium catalyst, 1 mmol of potassium carbonate, 0.75 mmol of 2,5-dimethoxyaniline in a Schlenk reaction tube, double-tube tube was purged with nitrogen, repeated three times, and then opened again. Nitrogen valve, add 2 ml of freshly distilled tetrahydrofuran, and close the valve. The tube was stirred at room temperature for 10 minutes and then placed at 110 ° C for 24 hours. After the completion of the reaction, TLC was plated, THF was evaporated, water was added, and water was added, and the mixture was extracted three times with ethyl acetate, and dried over anhydrous magnesium sulfate, and then evaporated to dryness to give the product white crystals: 0.385 mmol (104.5 mg). The product was N-(2,6-dimethoxyphenyl)-3-methylbenzamide in 77percent yield.
The synthetic route of 2734-70-5 has been constantly updated, and we look forward to future research findings.