Synthetic Route of 101-84-8,Some common heterocyclic compound, 101-84-8, name is Diphenyl oxide, molecular formula is C12H10O, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Example 12 (comparative)Decabromodiphenyl ether – Bromination of Deca completely dissolved in bromine.; The solubility of Deca in bromine was determined as 2.64 g Deca in 100 g bromine at 200C.To a 1 liter round bottomed flask equipped with a mechanical stirrer, a dropping funnel, a thermocouple and a reflux condenser was added 22 g of non milled Deca (content 97.1 %) and 1642 g bromine to produce a 1.32 % solution. AlBr3, 14.1 g, was added and the mixture was heated at reflux for 5 hours. After cooling to room temperature, water, 250 ml, was carefully added. The bromine was distilled and an additional 520 g of water was added. The solid was filtered and dried and consisted of 99.6 % Deca.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route Diphenyl oxide, its application will become more common.