In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 109-85-3 as follows. Formula: C3H9NO
Ligand 1b was prepared according to the method described for 1a using 2-(methoxy)ethylamine (0.39 mL, 4.54 mmol) and 1- methyl-1H-imidazole-2-carbaldehyde (0.455 g, 4.13 mmol) and isolated as a pale yellow oil in 92% yield. 1H NMR (300 MHz, CD2Cl2): d(ppm) 8.26 (s, 1H), 7.04 (s, 1H), 6.94 (s, 1H), 3.95 (s, 3H), 3.75e3.68 (m, 2H), 3.67e3.60 (m, 2H), 3.33 (s, 3H). 13C{1H} NMR (75 MHz, CD2Cl2): d(ppm) 154.96, 143.59, 129.32, 125.12, 72.53, 61.64, 58.86, 35.46. FT-IR (cm 1): 2875m, 1650s (nC]N), 1518w, 1475m, 1437m, 1366w, 1287m, 1236w, 1191w, 1118s, 1026w, 955w, 919m, 802m, 757m, 708m, 690m, 558w, 473w.
According to the analysis of related databases, 109-85-3, the application of this compound in the production field has become more and more popular.
Reference:
Article; Boudier, Adrien; Breuil, Pierre-Alain R.; Magna, Lionel; Olivier-Bourbigou, Helene; Braunstein, Pierre; Journal of Organometallic Chemistry; vol. 718; (2012); p. 31 – 37,7;; ; Article; Boudier, Adrien; Breuil, Pierre-Alain R.; Magna, Lionel; Olivier-Bourbigou, Helene; Braunstein, Pierre; Journal of Organometallic Chemistry; vol. 718; (2012); p. 31 – 37;,
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