Application of 24332-20-5, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 24332-20-5 as follows.
EXAMPLE 19 1-(2-Oxa)propyl-2-acetyl-6-methoxy-1,2,3,4-tetrahydro-beta-carboline. Formula: C1,H20 N2 O3 M=288.34 g.mol-1 To 5-methoxytryptamine (256 mg) dissolved in water (9 ml) are successively added hydrochloric acid (0.1 ml) and 1,1,2-trimethoxyethane (0.17 ml). The mixture is heated at reflux for 3 h. The medium is then diluted with hydrochloric acid solution (0.5 N, 40 ml). The aqueous phase is washed with ethyl acetate and then treated with 30% sodium hydroxide solution until the pH is basic. The mixture is then extracted three times with chloroform. After evaporation, 1-(2-oxo)propyl-6-methoxy-1,2,3,4-tetrahydro-beta-carboline is obtained.
According to the analysis of related databases, 24332-20-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Cemaf; Laboratories Besins Iscovesco; US6048868; (2000); A;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem