Some tips on 4316-51-2

According to the analysis of related databases, 4316-51-2, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 4316-51-2, name is 4-Methoxytriphenylamine, This compound has unique chemical properties. The synthetic route is as follows., Formula: C19H17NO

General procedure: Ni(cod)2 (3.4 mg, 0.025 mmol), ICy¡¤HBF4 (4.0 mg, 0.025 mmol), NaOtBu (48 mg, 0.50 mmol) and toluene (0.50 mL) were added to a 10 mL-sample vial with a Teflon-sealed screwcap in a glovebox filled with nitrogen. The resulting mixture was stirred at room temperature for 3 min. An aryl methyl ether (0.25 mmol) in toluene (0.50 mL) and AlMe3 (1.8 M in toluene solution, 0.14 mL, 0.25 mmol) were then added to the vial and the screw cap was closed. The contents of the vial were stirred at 80 C for 6 or 18 h. The reaction mixture was cooled to room temperature, and the crude mixture was then treated with EtOH. The resulting mixture was filtered through a pad of silica gel, and then analyzed by GC. The filtrate was concentrated in vacuo to give a residue, which was purified by flash column chromatography over silica gel.

According to the analysis of related databases, 4316-51-2, the application of this compound in the production field has become more and more popular.

Reference:
Article; Morioka, Toshifumi; Nishizawa, Akihiro; Nakamura, Keisuke; Tobisu, Mamoru; Chatani, Naoto; Chemistry Letters; vol. 44; 12; (2015); p. 1729 – 1731;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem