1515-89-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 1515-89-5, name is 1-Bromo-3-(methoxymethyl)benzene belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Reference Example 3 (2S)-3-(3-methoxymethylphenyl)propan-1,2-diol To a solution of the compound prepared in reference example 2 (19.5 g) in THF (10 ml) was added acetic acid (80 ml) and water (10 ml) and the mixture was heated to 60 C and stirred for 6 hours. To the mixture was added water (40 ml) and the mixture was cooled to room temperature, and the precipitate was removed by filtration. The filtrate was concentrated. The precipitate was removed again and the mixture was concentrated. From the obtained oil, the solvent was separated as azeotropic mixture with toluene to give the title compound (8.9 g) having the following physical data. TLC: Rf 0.64 (ethyl acetate: hexane = 2: 1).
The synthetic route of 1515-89-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; ONO PHARMACEUTICAL CO., LTD.; EP1114816; (2001); A1;,
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